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- W2040578052 abstract "Abstract Novel [{RhCl(CO)dppp} 2 ]‐catalyzed intramolecular carbonylative [2+2+1] cycloadditions of bis(phenylsulfonylallene) derivatives under CO, leading to the facile formation of bis(phenylsulfonyl)bicyclo[ n .3.0] frameworks ( n =4–6), have been developed. The terminal double bonds of both allenyl moieties served exclusively as the two π‐components. In particular, this newly developed method was shown to be a powerful tool for the construction of bicyclo[6.3.0]undecadienones, which have hardly been prepared by the known Pauson–Khand (‐type) reactions. The bicyclo[7.3.0]dodecadienone homologue (one extra carbon) could be formed in rather low yields. Alternatively, novel cycloisomerizations of bis(phenylsulfonylallene) derivatives with catalysis by the same Rh I complex under N 2 readily produced the 3,4‐dimethylene‐2,5‐bis(phenylsulfonyl)cyclononene and the corresponding cyclooctene and cycloheptene frameworks." @default.
- W2040578052 created "2016-06-24" @default.
- W2040578052 creator A5009931561 @default.
- W2040578052 creator A5013402633 @default.
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- W2040578052 creator A5057823553 @default.
- W2040578052 creator A5058280682 @default.
- W2040578052 creator A5065761459 @default.
- W2040578052 creator A5086935316 @default.
- W2040578052 date "2010-04-23" @default.
- W2040578052 modified "2023-10-18" @default.
- W2040578052 title "Rhodium(I)-Catalyzed Intramolecular Carbonylative [2+2+1] Cycloadditions and Cycloisomerizations of Bis(sulfonylallene)s" @default.
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- W2040578052 doi "https://doi.org/10.1002/chem.200903568" @default.
- W2040578052 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/20340116" @default.
- W2040578052 hasPublicationYear "2010" @default.
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