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• W2040582145 abstract "The crystallization behaviour of Fe74 Dy6 B20 and Fe70 Dy10 B20 amorphous alloys was carefully investigated by differential scanning calorimetry, Mossbauer spectrometry and x-ray diffraction up to 800 °C. Calorimetric studies were performed in limited temperature ranges that were progressively extended. For Fe74 Dy6 B20 , after partial crystallization into the tetragonal Fe3 B compound, the remaining amorphous part segregates into two amorphous `phases', respectively enriched and impoverished in dysprosium. Tetragonal Fe3 B further transforms into orthorhombic Fe3 B. Metastable Dy3 Fe62 B14 compound then forms from the Dy-impoverished amorphous fraction, and subsequent crystallization of the Dy1 + Fe4 B4 phase occurs in the Dy-enriched fraction. Finally, Dy3 Fe62 B14 decomposes into bcc iron, Dy1 + Fe4 B4 and iron borides. The nature of the first crystallization product suggests the existence of local environments of t-Fe3 B type for this Dy concentration. The crystallization process of Fe70 Dy10 B20 strongly differs from that of Fe74 Dy6 B20 . Segregation phenomena occur in the amorphous state prior to any crystallization. If the nature of the first crystallization product is assumed to be correlated with short-range order in the amorphous state, our results suggest that the local environments differ from those of Fe74 Dy6 B20 , as they probably involve dysprosium atoms. This behaviour would agree with a previous Mossbauer study performed on the as-quenched amorphous alloys, providing evidence for a structural modification of the iron environments in the rare earth concentration range 8-9 at.%." @default.
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• W2040582145 date "2000-03-30" @default.
• W2040582145 modified "2023-10-16" @default.
• W2040582145 title "Influence of the rare earth concentration on the crystallization process of Fe-Dy-B amorphous alloys. Study of Fe₇₄Dy₆B₂₀and Fe₇₀Dy₁₀B₂₀alloys" @default.
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• W2040582145 doi "https://doi.org/10.1088/0953-8984/12/15/313" @default.
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