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- W2040641385 abstract "Treatment of dimethylformamide 1a, diethylformamide 1b, 1-formylpiperidine 3a, 4-formylmorpholine 3b, and ethyl-phenylformamide 5 with sulphur tetrafluoride in the presence of potassium fluoride resulted in a direct conversion of the formyl group to the trifluoromethyl group to give excellent yields of dimethyl(trifluoromethyl)amine 2a, diethyl(trifluoromethyl )amine2b, 1-(trifluoromethyl)piperidine 4a, 4-(trifluoromethyl)morpholine 4b, and N-ethyl-N-(trifluoromethyl)aniline 6, respectively. The reaction pathway was investigated and the (trifluoromethyl)amines were characterised by spectral methods, elemental analyses, and hydrolysis to corresponding N-(fluoroformyl)amines 11." @default.
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- W2040641385 date "1983-06-01" @default.
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- W2040641385 title "Reaction of tertiary formamides with sulphur tetrafluoride. Direct synthesis of (trifluoromethyl)amines" @default.
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- W2040641385 doi "https://doi.org/10.1016/s0022-1139(00)85127-1" @default.
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