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- W2040674614 abstract "The synthesis and electrochemical characterisation of the following oxotitanium tetra-substituted phthalocyanines are reported: 1,(4)-(tetrabenzyloxyphthalocyaninato)titanium(IV) oxide (5a); 1,(4)-{tetrakis[4-(benzyloxy)phenoxy]phthalocyaninato}titanium(IV) oxide (5b); 2,(3)-(tetrabenzyloxyphthalocyaninato)titanium(IV) oxide (6a) and 2,(3)-{tetrakis[4-(benzyloxy)phenoxy]phthalocyaninato}titanium(IV) oxide (6b). The electrochemical characterisation of complexes octa-substituted with 4-(benzyloxy)phenoxy (9b), phenoxy (9c) and tert-butylphenoxy (9d) groups is also reported. The cyclic voltammograms of the complexes exhibit reversible couples I–III and couple IV is quasi-reversible for complexes 5a, 5b, 6a and 6b. The first two reductions are metal-based processes, confirmed by spectroelectrochemistry to be due to TiIVPc2−/TiIIIPc2− and TiIIIPc2−/TiIIPc2− redox processes and the last two reductions are ring-based processes due to TiIIPc2−/TiIIPc3− and TiIIPc3−/TiIIPc4−. Chronocoulometry confirmed a one-electron transfer at each reduction step. The electrochemistry of the above complexes is also compared to the previously reported 5c, 5d, 6c and 6d." @default.
- W2040674614 created "2016-06-24" @default.
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- W2040674614 date "2007-03-01" @default.
- W2040674614 modified "2023-09-26" @default.
- W2040674614 title "Electrochemical characterisation of tetra- and octa-substituted oxo(phthalocyaninato)titanium(IV) complexes" @default.
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- W2040674614 doi "https://doi.org/10.1016/j.electacta.2006.10.023" @default.
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