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- W2040690767 abstract "Time-of-flight secondary ion mass spectrometry (ToF-SIMS) and x-ray photoelectron spectroscopy (XPS) are used to characterize a newly synthesized glycosylated photoactivatable reagent designed for surface glycoengineering. The glycoaryldiazirine reagent MAD-Gal (N-[m-(3-(trifluoromethyl)diazirine-3-yl)phenyl]-4-(-3-thio(-1-D- galactopyrannosyl)-maleimidyl)butyramide) is immobilized with 350 nm light on diamond surfaces. The XPS atomic constituents and chemical shifts, as well as ToF-SIMS-specific characteristic fragments of the photoimmobilized molecule, are identified. The grafting on oxygen-containing sites previously observed for N-(m-(3-(trifluoromethyl)diazirine-3-yl)phenyl)-4-maleimido-butyramide (MAD) is confirmed. The difference in grafting efficiency for fresh and aged substrates indicates that other still unidentified reaction sites could be involved. The ToF-SIMS imaging is used to exhibit the ability to pattern the surface with the glycosylated aryldiazirine. © 1998 John Wiley & Sons, Ltd." @default.
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- W2040690767 date "1998-10-01" @default.
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- W2040690767 title "Part 2.N-[m-(3-(trifluoromethyl)diazirine-3-yl)phenyl]-4- (-3-thio(-1-D-galactopyrannosyl)-maleimidyl)butyramide (MAD-Gal) on diamond" @default.
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- W2040690767 doi "https://doi.org/10.1002/(sici)1096-9918(199810)26:11<793::aid-sia421>3.0.co;2-k" @default.
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