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- W2040752604 abstract "Poly(3-chlorothiophene) (PCT) films were synthesized electrochemically by direct oxidation of 3-chlorothiophene (CT) in mixed electrolytes of boron trifluoride diethyl etherate (BFEE) and trifluroacetic acid (TFA). The oxidation potential of 3-chlorothiophene in pure BFEE was measured to be only 1.54 V versus SCE. This value is much lower than that determined in neutral medium (2.18 V vs. SCE). The addition of TFA to BFEE can further decrease the oxidation potential of the monomer. The oxidation potential of CT in the mixed electrolyte of BFEE containing 30% TFA (by volume) was found to be as low as 1.16 V (vs. SCE). PCT films with the highest quality were obtained from the media of BFEE+10–15% TFA and they were characterized to have about 24–32 repeat units. The doping level and conductivity of PCT films also increased significantly by using the mixed electrolytes." @default.
- W2040752604 created "2016-06-24" @default.
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- W2040752604 date "2001-11-01" @default.
- W2040752604 modified "2023-10-11" @default.
- W2040752604 title "Low potential electrochemical polymerization of 3-chlorothiophene in mixed electrolytes of boron trifluoride diethyl etherate and trifluoroacetic acid" @default.
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- W2040752604 doi "https://doi.org/10.1016/s0022-0728(01)00632-5" @default.
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