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- W2040786860 abstract "A new series of polymeric nickel(II) complex cations of the formula [NiL4(N3)](PF6), for L=pyridine, 4-methyl-, 4-ethyl-, 3-chloro-, 3-bromo- and 3-hydroxy-pyridine, have been prepared and characterized. Solid state electronic spectra suggest six-coordinate nickel(II) in all complexes. IR spectral results reveal the existence of symmetrical azido ligands and PF6 − counter ions in these complexes. X-ray crystal structure determination has shown the complex for L=4-ethylpyridine (1) to contain a polymeric [NiL4(N3)]+ cation and PF6 − anions. In the cation each nickel(II) atom is coordinated by four nitrogen atoms from the pyridine ligands and two nitrogen atoms each from a μ-1,3 bridging azide giving rise to 1D polymeric chains of six-coordinate Ni(II) polyhedra. The azide ligand is symmetrical [N1N2=N2N3=1.152 and N1N2=1.164, N2N3=1.162 Å] and linear [NNN angles=178° and 180°] within the experimental error. The magnetic susceptibilities of 1 in the range of 2–300 K, have been measured and discussed." @default.
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- W2040786860 date "2002-08-01" @default.
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- W2040786860 title "A new series of 1D polymeric nickel(II) complex cations of pyridine derivative ligands with a single μ-1,3 azide bridge and X-ray crystal structure and magnetic properties of polymeric {[Ni(4-ethylpyridine)4(N3)n](PF6)n}" @default.
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- W2040786860 doi "https://doi.org/10.1016/s0277-5387(02)01061-6" @default.
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