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- W2040965513 abstract "13C CP/MAS spectra of 13C-labeled solution crystallized polyethylene at temperatures from −120 to 144°C are measured, in order to study changes of structure and molecular motion of the polymer with temperature variation. From these results, it was found that the non-crystalline 13C signal monotonically shifts downfield with a decrease of temperature, whereas the crystalline 13C signal does not change obviously with temperature. The maximum of the non-crystalline peak width appears at −30°C and that of the crystalline peak width appears at 110.4°C. The appearance of the maximum of the crystalline peak width is considered to correlate with the α-transition Another component besides the crystalline and non-crystalline components is found between 88 and 132.8°C, and is attributed to the interface and defects created in the heating process." @default.
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- W2040965513 date "1991-12-01" @default.
- W2040965513 modified "2023-09-27" @default.
- W2040965513 title "Structural characterization of solution-crystallized 13C-labeled polyethylene over a wide range of temperatures by means of high-resolution 13C NMR spectroscopy" @default.
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- W2040965513 doi "https://doi.org/10.1016/0022-2860(91)80074-e" @default.
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