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- W2040983486 abstract "Abstract Nine new mixed rare earth triple-decker complexes M 2 [TO(OH)PP](Pc) 2 [M = La…Dy, except Pm; H 2 Por = 5-(4-hydroxyphenyl)-10,15,20-tris(4-octyloxyphenyl)porphyrin] have been prepared by treating M(acac)[TO(OH)PP] with corresponding homoleptic unsubstituted bis(phthalocyaninato) rare earth complexes M(Pc) 2 in refluxing 1,2,4-trichlorobenzene (TCB). The origin of the electronic absorptions of these triple-decker complexes was tentatively revealed. For M 2 III [TO(OH)PP](Pc) 2 ], typical IR marker bands for the unsubstituted phthalocyanine dianion Pc 2− are strong bands at 1327–1329 cm −1 , and a weak band around 1370–1383 cm −1 . They can be assigned to pyrrole C C stretchings. Under excitation at 632.8 nm, typical Raman marker bands of the phthalocyanine dianions Pc 2− were observed at 1514–1526 cm −1 as medium band, resulting from the coupling of pyrrole C C and aza C N stretchings. The IR and Raman spectra for Ce 2 [TO(OH)PP](Pc) 2 are very slightly different from those of their other rare earth(III) counterparts. The nine complexes were also characterized by EA, MS and UV–vis spectra." @default.
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- W2040983486 date "2013-12-01" @default.
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- W2040983486 title "Synthesis and characterization of new mixed rare earth triple-decker complexes with A3B type [5-(4-hydroxyphenyl)-10,15,20-tris-(4-octyloxyphenyl)porphyrinato] and phthalocyaninato ligands" @default.
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- W2040983486 doi "https://doi.org/10.1016/j.dyepig.2013.05.014" @default.
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