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- W2041092607 abstract "The influence of dopants on the microstructure of quaternary Si-C-N-M-ceramics (M=B, P) is investigated. Monolithic amorphous ceramics are obtained by the polycocondensation of polysilazanes ((RR`SiNH)y) with the appropriate alkyl amide (M(NRR`)x) of boron or phosphorus and subsequent pyrolysis in argon atmosphere at 1000°C. The electron spectroscopic imaging method (ESI) in TEM reveals a homogeneous distribution of the elements Si, C, N and M. Upon annealing in nitrogen atmosphere at temperatures around 1400°C, crystallisation of the appropriate thermodynamically stable phases occurs. Heat treatment at temperatures up to 1800°C results in micro/nano-, nano/nano- or micro/microcrystalline microstructures with design-tailored properties which depend on the element M. Boron as dopant forms turbostratic boron nitride which coats the crystalline phases, inhibits the further crystal growth and thus leads to nanosize composite structure of the ceramics." @default.
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- W2041092607 date "1995-01-01" @default.
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- W2041092607 title "“Designing of Si3N4/SiC composite materials”" @default.
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- W2041092607 doi "https://doi.org/10.1016/0965-9773(95)00052-6" @default.
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