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• W2041208916 abstract "This paper describes a reliable method to selectively produce metastable α-form glycine crystals with a controlled size in batch cooling crystallization. Seeding had a large effect both on the polymorphism and the size distribution of the product crystals. In the case of sufficient seed loadings of the α-form crystals, the metastable α-form crystals were obtained selectively as a product. Simultaneously, the crystal size distribution became unimodal with no fine crystals. However, at low seed loadings, mixtures of both the metastable α- and stable γ-form crystals were obtained. The measurement of supersaturation transient suggested that the low supersaturation caused by the growth of sufficient seeds played a key role in suppressing nucleation of the metastable α- and γ-form crystals, whereas, with no seeding, only the stable γ-form crystals were obtained. The seeding technique presented here could be a general and practical method to produce metastable polymorphs with controlled crystal size." @default.
• W2041208916 created "2016-06-24" @default.
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• W2041208916 date "2003-11-22" @default.
• W2041208916 modified "2023-10-18" @default.
• W2041208916 title "Reliable and Selective Crystallization of the Metastable <i>α</i>-Form Glycine by Seeding" @default.
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• W2041208916 doi "https://doi.org/10.1021/cg034123h" @default.
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