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- W2041365600 abstract "Abstract A formal synthesis of (−)‐isoavenaciolide ( 1 ) by two different routes is reported. The first approach, leading to a key precursor 2 of (−)‐isoavenaciolide ( 1 ), features the stereoselective construction of the three contiguous stereogenic centers by Evans diastereoselective reduction ( d . e . = 80%) of β‐hydroxy ketone 8 . In the more efficient second approach, the nine‐step sequence leading to the key precursor 2 involves sequential ruthenium‐catalyzed hydrogenation reactions of β‐keto ester 4 and β‐hydroxy ketone 14 to form the two hydroxyl groups with an excellent control of the anti stereochemistry ( d . e . = 99%). (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)" @default.
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- W2041365600 date "2004-05-12" @default.
- W2041365600 modified "2023-09-25" @default.
- W2041365600 title "An Efficient Ruthenium‐Catalyzed Formal Synthesis of (−)‐Isoavenaciolide" @default.
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- W2041365600 doi "https://doi.org/10.1002/ejoc.200400047" @default.
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