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- W2041591239 abstract "Three reactions leading to the cleavage of the metal-metal bond in Ru 2 5+ complexes are described. The reaction of [Ru 2 (O 2 CMe) 4 -(thf) 2 ][BF 4 ] with CNC 6 H 11 leads to the formation of [Ru(CNC 6 H 11 ) 6 ][BF 4 ] 2 ( 1 ), reacting the same Ru 2 compound with [ N -nBu 4 ]-[SCN] leads to the isolation of [ N -nBu 4 ] 3 ]Ru(NCS) 6 ] ( 2 ), and the reaction between [Ru 2 (chp) 4 (thf)][CF 3 SO 3 ] and PMe 3 leads to the isolation of [Ru( O,N -chp)(PMe 3 ) 4 ][CF 3 SO 3 ] ( 3 ). Products 1 and 3 were structurally characterized and have the following crystallographic parameters; crystals of 1 are triclinic, space group P l (No. 2), with a=9.649(1), b=10.547(2), c=12.778(2) A ̊ , α =109.55(3), β =102.716(9), γ =98.74(2)°, Z =1; those of 3 are orthorhombic, space group P 2 1 2 1 2 1 (No. 19) with =9.790(2), b =10.134(4), c=29.722(4) A ̊ , Z=4 ." @default.
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- W2041591239 date "1998-07-01" @default.
- W2041591239 modified "2023-09-24" @default.
- W2041591239 title "Three reactions of Ru25+ compounds of the paddlewheel type that lead to cleavage of the RuRu bond" @default.
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- W2041591239 doi "https://doi.org/10.1016/s0020-1693(98)00136-4" @default.
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