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- W2041781254 abstract "We report on the temperature dependence of the nanostructure of thin block copolymer films, as studied using in situ grazing-incidence small-angle x-ray scattering (GISAXS). We focus on spin-coated poly(styrene-b-butadiene) diblock copolymer thin films featuring lamellae perpendicular to the substrate. In situ GISAXS measurements elucidate the structural changes during heat treatment at temperatures between 60 and 130 °C. Thermal treatment below 100 °C does not destroy the perpendicular lamellar order. In contrast, treatment between 105 and 120 °C leads to a broad distribution of lamellar orientations which only partially recovers upon subsequent cooling. Treatment at 130 °C leads to severe changes of the film structure. We attribute the change of behavior at 100 °C to the onset of the glass transition of the polystyrene block and the related increase of long-range mobility. Our results indicate that the perpendicular lamellar orientation for high molar mass samples is not stable under all conditions." @default.
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- W2041781254 date "2011-06-08" @default.
- W2041781254 modified "2023-10-18" @default.
- W2041781254 title "The effect of heat treatment on the internal structure of nanostructured block copolymer films" @default.
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- W2041781254 doi "https://doi.org/10.1088/0953-8984/23/25/254213" @default.
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