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- W2041805129 abstract "In order to determine the copper content x of copper Chevrel compound CuxMo6S8−y(0⩽y⩽0.4) as a function of copper activity aCu and sulfur deficit y, a solid state electrochemical cell, Cu/Rb4Cu16I7Cl13/CuxMo6S8−y/Pt, was constructed and coulometric titration studies were made at 400 K. For the evaluation of the coulometric titration data, measurements were made on the electronic conductivity of copper-ion conductor Rb4Cu16I7Cl13. Also, a brief investigation was made on the condition of formation of single phase Chevrel CuxMo6S8−y with varying x and y at 1000°C. The structural change of CuxMo6S8−y with a change in x and y was studied by the X-ray diffraction method. It was found that x for constant aCu decreases with increasing y. The maximum value xmax of x in CuxMo6S8−y in equilibrium with metallic copper was found to be expressed by xmax=-(103)y+5. In the region of y<0.3, xmax exceeded 4, contrary to a presupposition that xmax is less than 4. X-ray analysis revealed that most of the copper Chevrel compounds denoted by CuxMo6S8 so far were sulfur deficient ones with y≅0.4. The importance of sulfur deficit on the properties of the copper Chevrel compound was emphasized." @default.
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- W2041805129 date "1984-01-01" @default.
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- W2041805129 title "Coulometric titration of copper in CuxMo6S8−y(0⩽y⩽0.4) with solid Cu-electrolyte Rb4Cu16I7Cl13" @default.
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- W2041805129 doi "https://doi.org/10.1016/0167-2738(84)90019-5" @default.
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