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- W2042019946 abstract "Es werden Modellreaktionen zur Synthese eines Catenans mit der molekularen Untereinheit 2 beschrieben. 4,6-Dialkylpyrogallol-trimethyläther lassen sich aus Pyrogallol-trimethylather (3) durch schrittweise Metallierung mit Butyllithium und Alkylierung mit Alkylhalogeniden herstellen. 4,6-Didodecylpyrogallol (8) wird mit Cyclohexanon zu 10 acetalisiert und nach Methylierung zu 11 zur Nitroverbindung 12 umgesetzt. Alkylation of Polyphenol Derivatives, II. 4,6-Di-n-alkylpyrogallol Trimethyl Ethers. Model Investigation toward the Directed Syntheses of Catenanes Model reactions for the synthesis of a catenane with the molecular subunit 2 are described. 4,6-Dialkylpyrogallol trimethyl ethers can be prepared from pyrogallol trimethyl ether (3) by stepwise metalation with butyllithium and alkylation with alkyl halides. 4,6-Didodecylpyrogallol (8) is acetalized with cyclohexanone to 10 and, after methylation to 11, converted to the nitro compound 12." @default.
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- W2042019946 date "1973-09-01" @default.
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- W2042019946 title "Alkylierung von Polyphenolderivaten, II. 4,6‐Di‐n‐alkylpyrogallol‐trimethyläther. Modellreaktionen zu gezielten Catenan‐Synthesen" @default.
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- W2042019946 doi "https://doi.org/10.1002/cber.19731060920" @default.
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