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• W2042029845 endingPage "2129" @default.
• W2042029845 startingPage "2125" @default.
• W2042029845 abstract "The utility of polydentate monoanionic [Zr2(OiPr)9]- in generating arene-soluble, unsolvated, mixed-metal Zr/Ce and Zr/Y complexes is described. The synthesis of other mixed-metal zirconium lanthanide complexes was also studied to explore the relationship of metal size to structure. Lanthanide trihalides react in THF with KZr2(OiPr)9 to form unsolvated dimers, [[Zr2(OiPr)9]LnCl2]2, with the larger metals, Ln = Ce (1), Ho (2), Y (3), and unsolvated monomers, [Zr2(OiPr)9]LnCl2, with the smaller elements, Ln = Er (4), Yb (5). The synthesis of a monomeric iodide analogue, [Zr2(OiPr)9]TmI2, 6, by reduction of Zr2(OiPr)8(iPrOH)2 with TmI2(DME)3 is also reported. In all of these complexes, the [Zr2(OiPr)9]- subunit is tetradentate. 1-6 are compared with related cyclopentadienyl halide complexes to evaluate the special features of the dizirconium nonaisopropoxide ligand versus cyclopentadienide." @default.
• W2042029845 created "2016-06-24" @default.
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• W2042029845 date "2000-04-20" @default.
• W2042029845 modified "2023-10-16" @default.
• W2042029845 title "Synthesis of Arene-Soluble Mixed-Metal Zr/Ce, Zr/Y, and Related {[Zr₂(OⁱPr)₉]LnX₂}<i>_n</i> Complexes Using the Dizirconium Nonaisopropoxide Ligand" @default.
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• W2042029845 doi "https://doi.org/10.1021/ic991272+" @default.
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