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- W2042055260 abstract "Kalium- und Rubidiumamidometallate, K3M(NH2)6 und Rb3M(NH2)6, des Europiums, Yttriums und Ytterbiums wurden durch Umsetzung der entsprechenden Metalle in überkritischem Ammoniak als Reaktionspartner und Lösungsmittel in gut kristallisierter Form erhalten. Die röntgenographische Strukturbestimmung belegt eine Reihe isotyper Verbindungen: K3Y(NH2)6, K3Yb(NH2)6, Rb3Eu(NH2)6 und Rb3Y(NH2)6. Mit diesen ist das Rb3Yb(NH2)6 strukturverwandt. Die Atomanordnungen in den fünf ternären Amiden werden vergleichend diskutiert. Ausserdem sind die Verbindungen durch ihre Infrarotspektren charakterisiert. Potassium and rubidium amidometallates of europium, yttrium and ytterbium, K3M(NH2)6 and Rb3M(NH2)6, were prepared in a well-crystallized form by the reaction of the corresponding metals in supercritical ammonia as reactant and solvent. X-ray structure determinations gave a series of isotypic compounds: K3Y(NH2)6, K3Yb(NH2)6, Rb3Eu(NH2)6 and Rb3Y(NH2)6. Rb3Yb(NH2)6 has a structure closely related to these. The atomic arrangements of these five ternary amides are compared with one another. In addition, they are characterized by their IR spectra." @default.
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- W2042055260 date "1982-05-01" @default.
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- W2042055260 title "Über kalium- und rubidiumamidometallate des Europiums, Yttriums und Ytterbiums, K3M(NH2)6 und Rb3M(NH2)6" @default.
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- W2042055260 doi "https://doi.org/10.1016/0022-5088(82)90062-5" @default.
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