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- W2042079244 abstract "Five one-component solvent-based adhesives (series C) prepared from ε-polycaprolactone polyurethane (PU) polymers were used to join unchlorinated and chlorinated synthetic vulcanized styrene-butadiene rubber. PU films were characterized by infra-red (i.r.) spectroscopy, differential scanning calorimetry (d.s.c.), wide angle X-ray diffraction (WAXD), gel permeation chromatography (g.p.c.) and advancing contact angle measurements. T-peel tests in styrene-butadiene rubber/PU/styrene-butadiene rubber joints were carried out. The experimental results obtained allowed a distinction of PU films of series C according to their different configuration, i.e. the relative fraction and distribution of hard to soft segments: (i) PU with a relatively low hard/soft segment ratio (C1, C2, C4); and (ii) PU with a relatively high hard/soft segment ratio (C3, C5). A correlation, which was different for unchlorinated and chlorinated rubber, between advancing contact angle measurements, hard/soft segment ratio and T-peel strength of rubber/PU joints was found. For chlorinated rubber/PU adhesive/chlorinated rubber joints, the PU films with the highest surface energy produced the highest T-peel strenght. Furthermore, an interaction between the carboxylic and chlorinated groups on the chlorinated rubber surface and the polyester and/or urethane groups of PU was probably produced, in such a way that the highest T-peel strength corresponds to the polyurethane with the highest relative amount of soft segments." @default.
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- W2042079244 title "Relevance of polyurethane configuration on adhesion properties" @default.
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- W2042079244 doi "https://doi.org/10.1016/0143-7496(94)90030-2" @default.
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