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• W2042102485 abstract "The existence of short-chain domains in heterogeneous bimodal PDMS networks has been confirmed visually, for the first time, through confocal fluorescence microscopy. The networks were prepared using a controlled reaction scheme where short PDMS chains were reacted below the gelation point into hyperbranched structures using a fluorescent silicone compatible cross-linker. The formation of the hyperbranched structures was confirmed by FTIR, 1H-NMR and size exclusion chromatography (SEC). The short-chain hyperbranched structures were thereafter mixed with long-chain hyperbranched structures to form bimodal networks with short-chain domains within a long-chain network. The average sizes of the short-chain domains were found to vary from 2.1 to 5.7 μm depending on the short-chain content. The visualised network structure could be correlated thereafter to the elastic properties, which were determined by rheology. All heterogeneous bimodal networks displayed significantly lower moduli than mono-modal PDMS elastomers prepared from the long polymer chains. Low-loss moduli as well as low-sol fractions indicate that low-elastic moduli can be obtained without compromising the network's structure." @default.
• W2042102485 created "2016-06-24" @default.
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• W2042102485 date "2014-01-01" @default.
• W2042102485 modified "2023-09-27" @default.
• W2042102485 title "Visualisation and characterisation of heterogeneous bimodal PDMS networks" @default.
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• W2042102485 doi "https://doi.org/10.1039/c3ra47522k" @default.
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