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- W2042123112 abstract "N-Methyl carbamate insecticides and carbamate metabolities are separated on octylsilane and cyanopropylsilane bonded packing with an acetonitrile-water gradient mobile phase. The eluted carbamates are detected at the nanogram and sub- nanogram levels with a fluorescence detector after in-line hydrolysis to methylamine and subsequent reaction with o-phthalaldehyde and 2-mercaptoethanol to form the fluorophore. Using this high-performance liquid chromatographic (HPLC) technique, no responce was observed for 182 pesticides including various amides, anilides, anilines, carboximides, N-methyl carbamates, triazines, ureas and other nitrogen-containing pesticides. The HPLC post-column fluoremetric system provides the resolution, sensitivity and selectivity desired for the determination of multicarbamate insecticide residues." @default.
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- W2042123112 date "1979-12-01" @default.
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- W2042123112 title "Resolution, sensitivity and selectivity of a high-performance liquid chromatographic post-column fluorometric labeling technique for determination of carbamate insecticides" @default.
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- W2042123112 doi "https://doi.org/10.1016/s0021-9673(00)85635-6" @default.
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