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• W2042390407 abstract "An electrochemical cell has been developed for in situ x-ray diffraction from a working electrode under clean conditions equivalent to ultrahigh vacuum conditions of 5×10−10 mbar. The substrate crystals can be prepared ex situ and transferred into the cell under protection of ultrapure water within a few seconds. The oxygen level in the electrolyte is reduced by continuous N2 flow to less than 0.2% compared to that of a fresh electrolyte. This can be done while rotating the cell by 360° about the surface normal. The electrode potential is accurately measured at the position of the crystal using a Luggin capillary and a standard reference electrode. We demonstrate the performance of our cell by in situ synchrotron x-ray diffraction measurements on ultrathin Co layers electrodeposited on Cu(001) in an aqueous H2SO4/CoSO4 solution." @default.
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• W2042390407 date "1998-04-01" @default.
• W2042390407 modified "2023-09-24" @default.
• W2042390407 title "Electrochemical cell for <i>in situ</i> x-ray diffraction under ultrapure conditions" @default.
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• W2042390407 doi "https://doi.org/10.1063/1.1148852" @default.
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