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• W2042527883 abstract "Vinyl(triphenylethynyl)silane ((ph-C≡C)3-Si-C=CH2) (VTPES) was synthesized by Grignard reaction. Its molecular structure was characterized by means of fourier transform infrared spectroscopy (FT-IR) and nuclear magnetic resonance (1H-NMR, 13C-NMR, and 29Si-NMR). Poly(vinyl(triphenylethynyl))silane (PVTPES) was prepared by thermal polymerization and the catalytic graphitization of PVTPES with nickel, and Fe2O3 was also investigated between 900°C and 1600°C under nitrogen atmosphere. The effects of heat-treatment temperature and catalyst concentration on graphitization behavior were analyzed by X-ray diffraction (XRD), high-resolution transmission electron microscopy (HRTEM) and Laser Raman spectroscopy (LR). The results show that the presence of the transition metals produced graphitized areas with three-dimensional stacking order, and the Fe2O3 was more effective than nickel for catalytic graphitization. The key factor to affect graphitization behavior of PVTPES was the heat-treatment temperature compared with the catalyst concentration." @default.
• W2042527883 created "2016-06-24" @default.
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• W2042527883 date "2012-11-01" @default.
• W2042527883 modified "2023-10-16" @default.
• W2042527883 title "Synthesis and Catalytic Graphitization of Silicon Containing Arylacetylenic Resin" @default.
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• W2042527883 doi "https://doi.org/10.1080/1536383x.2011.572312" @default.
• W2042527883 hasPublicationYear "2012" @default.
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