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- W2042928874 abstract "Layered mixed divalent metal phosphonates Mg1 − xZnx(O3PR)·H2O [with R = CH3, C2H3, C6H5] and Ni1 − xZnx(O3PR)·H2O [with R = CH3, C2H3, C6H5, (CH2)2COOH] have been prepared by heating, respectively, mixed divalent magnesium–zinc hydroxides and nickel–zinc hydroxides above the melting point of the phosphonic acid being used. A range of pre-formed mixed divalent metal hydroxides Mg1 − xZnx(OH)2 and Ni1 − xZnx(OH)2 with different ratios of Zn content (x = 0, 0.1, 0.25, 0.5) are obtained by isomorphous substitution of zinc into the, respective, Mg(OH)2 and Ni(OH)2 brucite-type structure: space group Pm1; a = 3.13–3.15 Å, c = 4.63–4.77 Å). The phosphonate materials have been characterized by X-ray powder diffraction, IR, TGA, and 31P MAS NMR. Mg1 − xZnx(O3PR)·H2O and Ni1 − xZnx(O3PR)·H2O crystallize in an orthorhombic system with space group Pmn21 with b = 5.55–5.69 Å, c = 4.71–4.86 Å and a varying according to the size of the organic group R." @default.
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- W2042928874 title "Synthesis and characterization of new layered mixed metal phosphonate materials magnesium–zinc phosphonates Mg1 – xZnx(O3PR)·H2O and nickel–zinc phosphonates Ni1 – xZnx(O3PR)·H2O using mixed divalent magnesium–zinc and nickel–zinc hydroxides" @default.
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- W2042928874 doi "https://doi.org/10.1039/b105559n" @default.
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