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- W2043000354 abstract "A high-performance liquid chromatographic method for the determination of sulphonamides in urine is reported. The drugs (sulphadiazine, sulphaguanidine, sulphamethizole, sulphamethoxazole, and sulphathiazole) were diazotized with nitrite and coupled with N-(1-naphthyl)ethylenediamine dihydrochloride in a sodium dodecyl sulphate (SDS) micellar medium. Separation of the sulphonamide azo dyes was performed on a C18 column with a 0.05 M SDS-2.4% pentanol mobile phase, which permitted the direct injection of the urine samples. The limits of detection were in the 0.1–0.3 μg/ml range." @default.
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- W2043000354 date "1995-08-01" @default.
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- W2043000354 title "Determination of sulphonamides in human urine by azo dye precolumn derivatization and micellar liquid chromatography" @default.
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- W2043000354 doi "https://doi.org/10.1016/0378-4347(95)00158-f" @default.
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