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- W2043103652 abstract "A fast and effective dynamic sonication assisted ethanol extraction method was developed for extracting phenolic acids from basil, oregano, rosemary, sage, spearmint and thyme of the Lamiaceae family. The results were compared with results obtained by conventional solvent extraction techniques. A comprehensive two-dimensional liquid chromatography (LC × LC) system interfaced to electrospray ionisation time-of-flight (TOF) mass spectrometry was then optimised for analysis and quantification of the herb extracts. The optimised LC × LC system employed a combination of C18 and cyano columns. The relative standard deviations for the retention times were better than 0.05% (rosmarinic acid 0.1%) and those for the peak areas 2–14% (2 mg/l, n = 3). Limits of detection were 18–90 ng/ml. The LC × LC–MS method was applied to the quantitative analysis of phenolic acids, and the results were compared with those obtained with conventional LC–MS." @default.
- W2043103652 created "2016-06-24" @default.
- W2043103652 creator A5026900535 @default.
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- W2043103652 date "2007-03-01" @default.
- W2043103652 modified "2023-10-18" @default.
- W2043103652 title "Comprehensive two-dimensional liquid chromatography in analysis of Lamiaceae herbs: Characterisation and quantification of antioxidant phenolic acids" @default.
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- W2043103652 doi "https://doi.org/10.1016/j.chroma.2007.01.090" @default.
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