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- W2043201620 abstract "Optically active 2-[(3-hydroxypropyl)sulfinyl]-1-(o-tolyl)imidazole (S)-2 was synthesized by kinetic resolution of (±)-2 with lipase and hydrolysis of the acetate (S)-3 with potassium carbonate. The reaction mixture of the lipase-catalyzed transesterification was converted to the phthalic acid derivative (R)-4, and this (R)-4 and the unreacted acetate (S)-3 were fractionated without use of column chromatography. The unrequired recovered alcohol (R)-2 was also racemized and (±)-2 was repeatedly submitted to the lipase-catalyzed transesterification." @default.
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- W2043201620 date "1997-11-01" @default.
- W2043201620 modified "2023-09-23" @default.
- W2043201620 title "Synthesis of a key intermediate, (S)-2-[(3-hydroxypropyl)sulfinyl]-1-(o-tolyl)imidazole, for the platelet aggregation inhibitor, OPC-29030 via lipase-catalyzed enantioselective transesterification" @default.
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- W2043201620 doi "https://doi.org/10.1016/s0957-4166(97)00536-3" @default.
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