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- W2043251505 abstract "Four n.m.r. methods that are especially useful for characterization of oligosaccharides are applied to the trisaccharide α-Neu5Ac-(2→3)-β-Gal-(1→4)-Glc (1). Three of these are two-dimensional, heteronuclear methods that provide chemical-shift correlation maps having much higher sensitivity than was previously possible, because they rely on indirect observation of 13C via1H detection. These methods are used to assign, completely, the 1H- and 13C-n.m.r. spectra of both anomers of the trisaccharide. In addition to these two-dimensional methods, a one-dimensional method is used to measure 1H-1H coupling-constants accurately within each sugar ring. The values of the coupling constants thus measured for 1 are evidence that the conformations of the individual sugar rings are not affected by linkage into the trisaccharide." @default.
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- W2043251505 date "1987-08-01" @default.
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- W2043251505 title "Application of new, high-sensitivity, 1 H- 13 C-N.M.R.-spectral techniques to the study of oligosaccharides" @default.
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- W2043251505 doi "https://doi.org/10.1016/0008-6215(87)80042-3" @default.
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