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• W2043662025 endingPage "2604" @default.
• W2043662025 startingPage "2597" @default.
• W2043662025 abstract "Three ferrocene derivatives, Li[FcBH3], Li2[1,1′-fc(BMe3)2] and Li2[1,1′-fc(BMe2pz)2] [Fc=(C5H5)Fe(C5H4), fc=(C5H4)2Fe, pz=pyrazolyl], have been synthesized and structurally characterized to investigate the interaction of the negatively charged sandwich complex with its Li+ counterion(s) in the solid state. Single crystals of Li[FcBH3] · (12-crown-4), obtained from a THF solution after addition of 12-crown-4, contain hexacoordinated Li+ ions, which are bonded to one molecule of crown ether and to two hydrogen atoms of the BH3 fragment. The compound Li2[1,1′-fc(BMe3)2] crystallized from THF as solvent-separated ion pairs with each Li+ being encapsulated by four THF molecules. Single crystals of Li2[1,1′-fc(BMe2pz)2] were grown from diethyl ether. In this compound, the lithium ions are coordinated by two solvent molecules, the pyrazolyl side-arm and the cyclopentadienyl ring. Thus, Li2[1,1′-fc(BMe2pz)2] can be regarded as a trinuclear segment of the polymeric structure [–(C5H4R)Li(C5H4R)Fe–]∞ with R=BMe2pz." @default.
• W2043662025 created "2016-06-24" @default.
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• W2043662025 date "2004-11-01" @default.
• W2043662025 modified "2023-09-27" @default.
• W2043662025 title "On the way to ferrocene-based multiple-decker sandwich complexes" @default.
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• W2043662025 doi "https://doi.org/10.1016/j.poly.2004.05.017" @default.
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