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- W2043671979 abstract "Treatment of radical precursor 15a having a vinyl sulfide moiety with Bu3SnH in the presence of AIBN in boiling benzene afforded exclusively the 6-exo cyclization product 16a, whereas similar treatment of the exo-methylene compound 15b gave a mixture of the 6-exo cyclization product 16b and the endo-olefin product 17 formed by a 1,5-hydrogen shift. Based on these findings, the synthesis of (−)-aphanorphine was achieved using a sulfur-directed 6-exo-selective aryl radical cyclization of 22." @default.
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- W2043671979 date "2003-10-01" @default.
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- W2043671979 title "Synthesis of (−)-aphanorphine using a sulfur-directed aryl radical cyclization" @default.
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