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- W2043730456 abstract "PbTe nanopowders were synthesised by a gas induced reduction (GIR) method using Pb(NO3)2 and TeO2 as raw materials and hydrazine as reductant at different temperatures. The nanopowders were characterised by X-ray diffraction (XRD) and field emission scanning electron microscope (FESEM) equipped with energy dispersive X-ray spectroscopy. The morphology of the PbTe powders varied with synthesis temperatures. As the synthesis temperature increased, the powder shape gradually changed from spherical to rod-like, i.e. the morphology of the powder can be controlled by adjusting the synthesis temperature. The spherical PbTe particles with diameter of 100 nm were synthesised at 348 K for 24 h, while PbTe nanorods with 200–300 nm in diameter and about 2 μm in length were prepared at 423 K for 24 h. Based on the experimental results and analysis, the growth mechanism of the PbTe nanopowders was proposed. The powders after cold pressing exhibit very high Seebeck coefficient of ∼405 μV K−1." @default.
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- W2043730456 date "2014-07-01" @default.
- W2043730456 modified "2023-09-27" @default.
- W2043730456 title "Synthesis and characterisation of PbTe thermoelectric nanopowders via a gas induced reduction route" @default.
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- W2043730456 doi "https://doi.org/10.1179/1432891714z.000000000652" @default.
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