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- W2043901630 abstract "The structure of primitive-cubic YbZrF7 has been determined using X-ray and neutron diffraction techniques. A unit cell (a = 4.07 Å, space group Pm3m) contains one formula unit of Yb0.5Zr0.5F3.5, with no ordering of cations, in materials prepared by rapid quenching from 1000°C. Metal and fluorine displacements from ideal sites are in accord with results previously obtained on Zr0.8Yb0.2F3.2O0.3. The separation between FF pairs bridging neighboring metal ions is similar to those observed in other complex zirconium fluorides. The metal displacements, metal-fluorine distances and fluorine-fluorine distances are discussed with respect to the formation and stability of disordered fluorine-excess ReO3-type phases. These materials are intermediate in character between phases such as monoclinic YbZrF7, with perfect order on both metal and nonmetal sublattices, and ZrF4-based glasses where there is disorder on the metal as well as on the fluorine sublattice. No ordering effects are observed on heating to near 200°C, but near 400°C there is a slow transformation to the monoclinic YbZrF7 structure." @default.
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- W2043901630 date "1981-10-01" @default.
- W2043901630 modified "2023-09-25" @default.
- W2043901630 title "The structure of cubic YbZrF7" @default.
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- W2043901630 doi "https://doi.org/10.1016/0022-4596(81)90266-8" @default.
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