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- W2043914157 abstract "Abstract Combination of two techniques, photoacoustic (PA) and differential scanning calorimetry (DSC), is a combination of quasi stationary thermodynamic DSC method and nonstationary dynamic PA method. Especially favorable and easy to realize is the combination with power compensated type of DSC. It has several advantages over the use of two techniques separately and allow to perform measurements simultaneously. The most obvious is simultaneous determination of thermodynamic properties such as specific heat, heat of transition and dynamic properties such as effusivity, thermal conductivity at the different phase transitions and complex specific heat at the glass transition. Unlike other temperature modulated techniques PA–DSC is especially suitable for studying polymer materials since their low thermal conductivity is an additional advantage. Conditions for simultaneous measurements are examined. It is proved that the combination of two techniques and necessary changes in construction do not essentially change adequate work of the instrument. A little disbalance of DSC operation due to the construction change can be corrected simply by recalibration. The procedures for testing and calibration for the proper operation of the combined PA–DSC are given together with some details of experimental methodology. Several measurements could serve as examples of widespread applicability of PA–DSC to study different types of phase transitions as well as time dependent processes such as glass transition." @default.
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- W2043914157 date "1999-05-01" @default.
- W2043914157 modified "2023-09-27" @default.
- W2043914157 title "A combined photoacoustic DSC for simultaneous temperature modulated measurements: does it really work?" @default.
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- W2043914157 doi "https://doi.org/10.1016/s0040-6031(99)00029-5" @default.
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