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- W2043918215 abstract "The ultrafine bio-glass powder of Si-Al-Ca-P-F - polynary system was prepared by sol-gel method with organic and inorganic compounds such as Si (OC 2 H 5 ) 4 , (C 2 H 5 ) 3 PO 4 , Ca (NO 3 ) 2 ·4H 2 O, Al (NO 3 ) 3 ·9H 2 O and NH 4 F. The powder was heat-treated at the different temperature in the range from 200 to 900°C and its crystallized transition was ascertained. The morphology, composition, structure state and crystallized behavior of the glassy powder were characterized by means of TEM, XRD, EDS, DSC-TG, FT-IR etc methods and compared with the glassy powder of the same system by melting-quenching and liquid precipitation. The results show that the powder containing elements Si, Al, Ca, P, F and O belongs to typical amorphous state, and is composed of the near spherical particles with the size from 100 to 400nm; The transition temperature of glass was about 580°C, and the crystallized phase CaF 2 precipitate firstly above 600°C; A series of crystallized phases Ca 5 (PO 4 ) 3 F and Ca 5 (PO 4 ) 2 SiO 4 were separated sequentially with increasing temperature; The network structure of glass is similar to that of melt-quenching or liquid precipitation glass." @default.
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- W2043918215 date "2011-11-01" @default.
- W2043918215 modified "2023-09-27" @default.
- W2043918215 title "Characterization of Ultrafine Glassy Powder for Al-Si-Ca-P-O-F Polynary System by Sol-Gel Method" @default.
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- W2043918215 doi "https://doi.org/10.4028/www.scientific.net/amr.412.138" @default.
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