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- W2043930907 abstract "JV 485 [14C-Ph] and JV 485 [14C-Py] were synthesized in seven steps in 35% and 44% overall yields, respectively, utilizing the same reaction schemes. The key step in each of the syntheses is a one pot Mid-Century Oxidation (1) of an aromatic methyl group to a carboxylic acid. The 14C radiolabeled syntheses of two isolated metabolites of JV 485 were also completed. Preparation of the JV 485 [phenyl-14C(U)] amide was completed in 62% yield from 2-chloro-5-[4-bromo-1-methyl-5-trifluoromethyl)-1H-pyrazol-3-yl]-4-fluorobenzoic acid [ring-14C(U)], 9. Preparation of the JV 485 [phenyl-14C(U)] desmethyl acid 13 was accomplished in 18% overall yield in four steps from 3-(4-chloro-2-fluoro-5-methylphenyl [ring-14C(U)])-5-(trifluoromethyl)-1H-pyrazole, 4. Copyright © 2000 John Wiley & Sons, Ltd." @default.
- W2043930907 created "2016-06-24" @default.
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- W2043930907 date "2000-01-01" @default.
- W2043930907 modified "2023-09-25" @default.
- W2043930907 title "The radiolabeled syntheses of JV 485, a herbicide candidate for winter wheat" @default.
- W2043930907 doi "https://doi.org/10.1002/1099-1344(200006)43:7<645::aid-jlcr349>3.0.co;2-6" @default.
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