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- W2043979799 abstract "The crystal structure of sinigrin (potassium myronate), KC_(10)H_(16)NO_9S_2. H_2O, has been refined on thebasis of three-dimensional intensity data collected on an automated diffractometer. The final agreementindex is 0·056 for 1906 reflections, and the estimated standard deviations in the atomic coordinates of theC, N, and 0 atoms are about 0·004 A. The absolute configuration of the anion was confirmed fromanomalous dispersion effects. The crystals are orthorhombic with space group P212121. The unit-celldimensions of a new crystal are ɑ = 8·265 (1), b = l1·440(3), and c = 17·757 (3)A. An appreciable increasein the length of the c axis occurred during irradiation of the crystal. In addition, the vinyl groupof the myronate ion appears to undergo large thermal motions. The distances between vinyl groups ofadjacent myronate ions are such that a photopolymerization reaction between them would be possible,which might explain these two observations." @default.
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- W2043979799 date "1970-07-15" @default.
- W2043979799 modified "2023-10-02" @default.
- W2043979799 title "Refinement of the crystal structure of sinigrin" @default.
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- W2043979799 doi "https://doi.org/10.1107/s0567740870003539" @default.
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