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• W2044003852 abstract "We have investigated the dynamic mechanical behavior of two cross-linked polymer networks with very different topologies: one made of backbones randomly linked along their length; the other with fixed-length strands uniformly cross-linked at their ends. The samples were analyzed using oscillatory shear, at very small strains corresponding to the linear regime. This was carried out at a range of frequencies, and at temperatures ranging from the glass plateau, through the glass transition, and well into the rubbery region. Through the glass transition, the data obeyed the time−temperature superposition principle, and could be analyzed using WLF treatment. At higher temperatures, in the rubbery region, the storage modulus was found to deviate from this, taking a value that is independent of frequency. This value increased linearly with temperature, as expected for the entropic rubber elasticity, but with a substantial negative offset inconsistent with straightforward enthalpic effects. Conversely, the loss modulus continued to follow time−temperature superposition, decreasing with increasing temperature, and showing a power-law dependence on frequency." @default.
• W2044003852 created "2016-06-24" @default.
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• W2044003852 date "2004-01-27" @default.
• W2044003852 modified "2023-09-27" @default.
• W2044003852 title "Dynamic Shear Modulus of Isotropic Elastomers" @default.
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• W2044003852 doi "https://doi.org/10.1021/ma035060e" @default.
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