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- W2044029319 abstract "Unusual metal carboxylates that are liquids at room temperature have been synthesized and applied to the preparation of nickel ferrite. These salts Ni(MEEA)2·0.5H2O and Fe3O(MEEA)7·5.5(H2O) bear the polyether carboxylate anion 2-[2-(2-methoxyethoxy)ethoxy]acetate (MEEA = CH3OCH2CH2OCH2CH2OCH2CO2-). They may be utilized for the low-temperature preparation of nickel ferrite by using Ni(MEEA)2·0.5H2O to coat Fe2O3 powders with a continuous film of NiO. Upon heating this material to 800 °C, a remarkable solid-state reaction occurs to puff the precursor particles into broccoli floret-like collections of very small particles. A homogeneous precursor solution for nickel ferrite may be prepared via dissolution of Ni(NO3)2 in Fe3O(MEEA)7·5.5(H2O). This precursor solution yields a metastable amorphous NiFe2O4 phase at 300 °C which undergoes an exothermic crystallization at 374 °C with an energy change of −126.1 kJ/mol." @default.
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- W2044029319 date "1998-04-28" @default.
- W2044029319 modified "2023-09-26" @default.
- W2044029319 title "Preparation of Nickel Ferrite Using Liquid Metal Carboxylates" @default.
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- W2044029319 doi "https://doi.org/10.1021/cm970360u" @default.
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