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• W2044133091 abstract "Interaction of the [α-H 2 P 2 W 12 O 48 ] 12− with the Fe III in aqueous solution results in the formation of an equatorial tri-iron substituted Wells–Dawson compound K 4 Cs 2 Fe 2 [P 2 W 15 (FeOH) 3 O 59 ]·22H 2 O, with antiferromagnetism and bifunctional electrocatalytic activities. Interaction of the hexa-lacunary polyanion precursor [α-H 2 P 2 W 12 O 48 ] 12− and the Fe III in aqueous solution results in the formation of an equatorial tri-iron substituted Wells–Dawson type compound, K 4 Cs 2 Fe 2 [P 2 W 15 (FeOH) 3 O 59 ]·22H 2 O ( 1 ). Compound 1 was characterized by IR, elemental, single-crystal X-ray diffraction, thermogravimetric, magnetic, as well as electrochemical analysis. The polyoxoanion [P 2 W 15 (FeOH) 3 O 59 ] 12− can be viewed as a derivative of the parent polyoxoanion [α-P 2 W 18 O 62 ] 6− by removal of three belt W O groups and then inhabited by three Fe OH groups. The compound 1 -modified carbon paste electrode ( 1 -CPE) presents good electrocatalytic activity not only toward the reduction of nitrite which is attributed to the function of tungstophosphate, but also toward the oxidation of ascorbic acid which is primarily attributed to the function of Fe III . The magnetic properties of 1 have been studied by magnetic susceptibility and fitted according to an isotropic exchange model. Compound 1 exhibits strong antiferromagnetic spin exchange interactions between the Fe III centers." @default.
• W2044133091 created "2016-06-24" @default.
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• W2044133091 date "2010-03-01" @default.
• W2044133091 modified "2023-09-24" @default.
• W2044133091 title "An equatorial tri-iron substituted Wells–Dawson type tungstophosphate with magnetic and bifunctional electrocatalytic properties" @default.
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• W2044133091 doi "https://doi.org/10.1016/j.ica.2009.11.029" @default.
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