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- W2044171340 abstract "Abstract 1,3-Bis(1 H -benzimidazol-2-yl)-2-oxapropane ( L ) complexes with ZnX 2 (X = Cl − , Br − , I − , CH 3 COO − , NO 3 − , ClO 4 − ) ( 1 – 6 ) were synthesized and characterized by elemental analysis, molar conductivity, TGA, FT-IR, NMR, ESI-MS and fluorescence spectroscopy. In addition, the crystal structure of [1,3-bis(1 H -benzimidazol-2-yl)-2-oxapropane- κ 2 N,N ′]dibromozinc(II) { 2 , [Zn( L )Br 2 ]}, is reported. The Zn(II) ion has a tetrahedral environment in the chelate complex. The ZnCl 2 complex ( 1 ) is structurally different from the others: It shows a broad signal at 7.28 ppm in the 1 H NMR spectra assigned to two coordinated water molecules. The very low solubility of the acetate complex ( 4 ) leads us to suggest a polymeric structure with [Zn 2 ( μ -OAc) 4 ( L ) 2 ] n paddlewheel units. The ligand shows from two to four emission bands in polar solvents. Compared to the ligand, the complexes show weak fluorescence intensity in ethanol and exhibit red- or blue-shift." @default.
- W2044171340 created "2016-06-24" @default.
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- W2044171340 date "2014-09-01" @default.
- W2044171340 modified "2023-10-18" @default.
- W2044171340 title "Synthesis and spectral characterization of 1,3-bis-(1 H -benzimidazol-2-yl)-2-oxapropane complexes with various Zn(II) salts" @default.
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- W2044171340 doi "https://doi.org/10.1016/j.ica.2014.07.036" @default.
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