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- W2044233308 abstract "Sterically hindered nickel- tripyrrins [Ni(trpy)X] with different di-, tri- and tetradentate anions X have been prepared with the aim of finding coordination polymers formed by self-association. The syntheses were performed by simple ligand-exchange reactions and proceeded successfully with the pseudohalides CN−, OCN−, SCN−, SeCN−, N(CN)2− (dicyanoamido, dca) and C(CN)3− (tricyanomethanido, tcm), the cyanidometallates [Ag(CN)2]− and [Ni(CN)4]2− and the salicylate anion (sal−). X-ray crystallographic analyses revealed that the complexes with cyanido and isocyanato ligands, as well as the compound with a salicylato ligand, are prototypes for structurally distinct monomeric species in the solid state, whereas one-dimensional coordination polymers or supramolecular three-dimensional networks are formed from all other combinations. The polymeric compounds display a variety of individual pillar and network architectures with functionalised pores and clefts and with the Ni(trpy) fragments in different relative orientations. Hydrogen bonding and π stacking were found to be additional structure-directing effects, which increased the structural complexity of the system. The Ni(trpy) subunit has thus been proven to be a versatile building block for the construction of supramolecular assemblies and metal organic frameworks (MOFs) from pentacoordinate NiII ions." @default.
- W2044233308 created "2016-06-24" @default.
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- W2044233308 date "2007-01-02" @default.
- W2044233308 modified "2023-10-16" @default.
- W2044233308 title "Pillars, Layers, Pores and Networks from Nickeltripyrrins: A Porphyrin Fragment as a Versatile Building Block for the Construction of Supramolecular Assemblies" @default.
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- W2044233308 doi "https://doi.org/10.1002/chem.200601296" @default.
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