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- W2044238296 abstract "Bis(toluene)chromium fulleride, [Cr(C(7)H(8))(2)]C(60), has been synthesized as a black microcrystalline powder from C(60) and [Cr(C(7)H(8))(2)] in toluene. [Cr(C(7)H(8))(2)]C(60) is an ionic compound in which the fullerene is negatively charged and the bis(toluene)chromium molecule positively charged. At T = 250 K a reversible first-order phase transition from a primitive cubic high-temperature phase to a triclinic low-temperature phase occurs. The high-temperature phase [Pm3 macro m, a = 9.9840 (1) A, T = 295 K] is composed of dynamically disordered fulleride anions and bis(toluene)chromium(I) cations in a CsCl-type arrangement. The triclinic low-temperature modification [P1 macro, a = 13.6414 (8), b = 13.8338 (7), c = 13.8548 (7) A, alpha = 91.830 (3), beta = 116.776 (2), gamma = 119.333 (2) degrees, T = 235 K] consists of ordered C(60) dimers and two crystallographically distinct bis(toluene)chromium entities." @default.
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- W2044238296 date "2002-05-29" @default.
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- W2044238296 title "Reversible dimerization of C<sub>60</sub> molecules in the crystal structure of the bis(arene)chromium fulleride [Cr(C<sub>7</sub>H<sub>8</sub>)]<sub>2</sub>C<sub>60</sub>" @default.
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- W2044238296 doi "https://doi.org/10.1107/s0108768102001970" @default.
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