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- W2044416401 abstract "The unsymmetrical ligand H 2 bpabza has been prepared in good yield using TBAB as the reaction medium. The M(bpabza) complexes have been synthesized by electrochemical oxidation of anodic metals (M = Cu, Zn) in an acetonitrile solution of H 2 L. X-ray analysis revealed that the Cu(II) ion adopts a distorted square pyramidal (4 + 1) coordination in the solid state. The direct electrosynthesis of neutral copper(II) and zinc(II) complexes of a new unsymmetrical carboxamide ligand, N , N ′-bis(2-pyridinecarboxamide)-2-aminobenzylamine (H 2 bpabza) derived from 2-pyridinecarboxylic acid and 2-aminobenzylamine, was accomplished by electrochemical oxidation of anodic metals (copper and zinc) in an acetonitrile solution of the ligand. These compounds were characterized by elemental analyses and different spectroscopic methods. The crystal and molecular structures of the ligand, H 2 bpabza, and its copper complex, Cu(bpabza), were determined by X-ray diffraction. The copper atom adopts a distorted square-pyramidal (4 + 1) CuN 2 N′N″O coordination geometry with bpabza 2− acting as a dianionic tetradentate ligand furnishing four N atoms in the base, with the O atom of a carbonyl group from an adjacent molecule in the apical position of the coordination environment." @default.
- W2044416401 created "2016-06-24" @default.
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- W2044416401 date "2015-01-01" @default.
- W2044416401 modified "2023-10-14" @default.
- W2044416401 title "Direct electrochemical synthesis of copper(II) and zinc(II) complexes of the tetradentate ligand N,N′-bis(2-pyridinecarboxamide)-2-aminobenzylamine (H2bpabza). The crystal structures of the ligand and its Cu(II) complex" @default.
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- W2044416401 doi "https://doi.org/10.1016/j.poly.2014.08.065" @default.
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