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• W2044479964 abstract "Abstract The reaction of the title ligand N-(2-pyridyl)-3-phenyl-2-propene amide (O-N) with MX2 salts yields compounds of the type M(O-N)2X2 and [M(O-N)2(H2O)2]X2, which were characterized by elemental analysis, magnetic moments and IR and EPR spectroscopies. From the IR spectra the ligand is found to be bidentate via the pyridyl nitrogen and the amide oxygen, except in [Pd(O-N)2Cl2] where only the pyridyl ring is coordinated. The magnetic moments, IR spectra and thermograms of the M(O-N)2(NO3)2·3H2O compounds [M = nickel(II), cobalt(II)] are consistent with the presence of trans-[M(O-N)2(H2O)2]2+ ions, similar to the trans-[Zn(O-N)2(CH3OH)2]2+ species observed earlier. The EPR spectra of the trans-Cu(O-N)2X2 compounds (X = NO3−, CF3SO3−) indicate an elongated octahedral coordination with equatorial bidentate (O-N) ligands and solvent molecules or anions in axial sites. The solid-state spectra reveal the presence of more than one type of copper(II) centre. The crystal structure of trans-Cu(O-N)2(CF3SO3)2 was determined by X-ray diffraction. The unit cell contains two types of discrete trans-Cu(O-N)2(CF3SO3)2 molecules, in which bidentate (O-N) ligands are strongly bonded to the equatorial sites of a tetragonally distorted octahedron. The axial positions are filled by" @default.
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• W2044479964 date "1993-03-01" @default.
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• W2044479964 title "N-(2-pyridyl)-3-phenyl-2-propene amide (O-N) complexes fo copper(II), nickel(II), cobalt(II) and palladium(II). Crystal and molecular structure of Cu(O-N)2(CF3SO3)2" @default.
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• W2044479964 doi "https://doi.org/10.1016/s0277-5387(00)83397-5" @default.
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