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- W2044486722 abstract "Reaction of the dilithium salt of the Schiff-base N,N′-o-phenylene-bis(3,5-di-tert-butyl-salicylidene-imine) (tBu4salophenH2) with 1 equiv. of ZrCl4(THF)2 in toluene at −78 °C affords the dichloro complex ZrCl2[C6H4-1,2-{NCH-(3,5-tBu2C6H2-2-O)}2], isolated as a mixture of the C2v-(3a) and C2-(3b) symmetry isomers. Thermodynamic and kinetic parameters for the equilibrium between 3a and 3b have been determined and studied by 1H NMR spectroscopy. Reactions of ZrCl2[C6H4-1,2-{NCH-(3,5-tBu2C6H2-2-O)}2] with alkylating reagents gave an intractable, unidentified mixture of products from which the NMR spectra in C6D6 solution are unusable." @default.
- W2044486722 created "2016-06-24" @default.
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- W2044486722 date "2006-09-01" @default.
- W2044486722 modified "2023-10-11" @default.
- W2044486722 title "A zirconium dichloro complex supported by an ancillary stereorigid tetradentate bis(phenoxo-imino) Schiff-base-donor ligand: Evidence for a conformational equilibrium between two solution stereoisomers" @default.
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- W2044486722 doi "https://doi.org/10.1016/j.jorganchem.2006.05.025" @default.
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