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- W2044658449 abstract "Abstract Amorphous Si 37 C 32 N 31 and Si 37 C 29 N 34 ceramics were produced by pyrolysis of a polyhy-dromethylsilazane precursor. Their structure was investigated by X-ray and neutron diffraction. Wide angle diffraction showed that the Si-atoms are preferentially bonded to nitrogen atoms, but also bonding to carbon atoms was found. This suggests that the excess carbon atoms form an amorphous graphite-like phase. Small angle scattering revealed that the ceramics are inhomogeneous. The evolution of the phase separation during annealing was investigated and it was concluded that amorphous Si 3 N 4 precipitates grow in the Si-C-N materials. The results are compared with previous results for amorphous Si 24 C 43 N 33 produced from a polysilylcarbodiimide precursor [1 - 3]." @default.
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- W2044658449 date "1998-04-01" @default.
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- W2044658449 title "Study of the Atomic Structure and Phase Separation in Amorphous Si-C-N Ceramics by X-Ray and Neutron Diffraction" @default.
- W2044658449 doi "https://doi.org/10.1515/zna-1998-3-405" @default.
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