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- W2044669603 abstract "Abstract The reaction of trans -1,2-diaminocyclohexane with enantiopure ( R )-2-formyl-1-phosphanorbornadiene ( 1 ) takes place with efficient kinetic resolution and gives an easily separable mixture of the corresponding ( S , S )-bis-imine ( 3 ) and ( R )-mono-imine ( 4 ). The absolute configuration of 3 has been established by X-ray crystal structure analysis. The coordination chemistry of enantiopure 3 with Pd(II), Rh(I), and Ru(II) has been investigated. The reaction of [PdCl 2 (cod)] mainly affords a binuclear complex 6 whose structure has been established by X-ray analysis. One PdCl 3 - unit is coordinated to one P and one PdCl + unit is tricoordinated to the other P and the two N. The two square planar units are parallel and the Pd⋯Pd distance is 3.1787(5) A. The reaction of [RhCl(cod)] 2 gives the very reactive tetracoordinate cationic [Rh(P 2 N 2 )] + species 7 which is able to activate one C–Cl bond of chloroform to give the dichloromethyl-Rh complex ( 8 ) whose octahedral structure has been ascertained by X-ray analysis." @default.
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- W2044669603 date "2005-03-01" @default.
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- W2044669603 title "The coordination chemistry of enantiopure diimines derived from 1-phosphanorbornadiene-2-carboxaldehydes" @default.
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- W2044669603 doi "https://doi.org/10.1016/j.jorganchem.2004.11.018" @default.
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