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• W2044693103 abstract "In this paper we demonstrate the feasibility of replacing KF for water content testing in bulk powders and tablets with at-line near infrared (NIR) or microwave resonance (MR) methods. Accurate NIR and MR prediction models were developed with a minimalistic approach to calibration. The NIR method can accurately predict water content in bulk powders in the range of 0.5-5% w/w. Results from this method were compared to a MR method. We demonstrated excellent agreement of both NIR and MR methods for powders vs. the reference KF method. These methods are applicable to in-process control or quality control environments. One of the aims of this study was to determine if a calibration developed for a particular product could be used to predict the water content of another product (with related composition) but containing a different active pharmaceutical ingredient (API). We demonstrated that, contrary to the NIR method, a general MR method can be used to predict water content in two different types of blends. Finally, we demonstrated that a MR method can be developed for at-line moisture determination in tablets." @default.
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• W2044693103 date "2011-06-01" @default.
• W2044693103 modified "2023-09-30" @default.
• W2044693103 title "Comparison of near infrared and microwave resonance sensors for at-line moisture determination in powders and tablets" @default.
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• W2044693103 doi "https://doi.org/10.1016/j.aca.2011.03.048" @default.
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