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- W2044843915 abstract "An ultrasound/vortex assisted dispersive liquid–liquid microextraction (USVADLLME) procedure coupled with gas chromatography–ion trap mass spectrometry (GC-IT-MS) is proposed for the rapid determination of seven phthalate esters in soft drinks and light alcoholic beverages (up to 6% alcohol by volume). Under the optimum conditions, the enrichment factors of the seven phthalate esters ranged from 205-fold to 315-fold for soft drinks and from 172-fold to 285-fold for light alcoholic beverages. The recoveries varied between 94.2% and 99.6% for soft drinks and 95.6% and 99.4% for light alcoholic beverages. The limits of detection were between 0.03 and 0.10 pg μL−1 and the limits of quantification were between 0.11 and 0.28 pg μL−1. The intra-day and inter-day precision expressed as the relative standard deviation varied between 2.9% and 5.1% and between 5.5% and 7.6%, respectively. The proposed USVADLLME-GC-IT-MS method was demonstrated to be simple, reproducible and practical for the determination of trace amounts of seven phthalate esters in soft drinks and light alcoholic beverages." @default.
- W2044843915 created "2016-06-24" @default.
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- W2044843915 date "2014-10-20" @default.
- W2044843915 modified "2023-09-25" @default.
- W2044843915 title "Fast determination of phthalate ester residues in soft drinks and light alcoholic beverages by ultrasound/vortex assisted dispersive liquid–liquid microextraction followed by gas chromatography-ion trap mass spectrometry" @default.
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- W2044843915 doi "https://doi.org/10.1039/c4ra08574d" @default.
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