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- W2044950905 abstract "Abstract The reaction between antimony trichloride and tetramethylammonium chloride in nitromethane gives transparent, irregular crystals of tetrakis(tetramethylammonium) octacosachlorooctaantimonate(III) [(CH 3 ) 4 N] 4 Sb 8 Cl 28 . Crystals are triclinic, space group P-1, a =11.846(2), b =12.217(2), c=14.120(3) A , α =95.71(3), β =101.39(3), γ =118.59(3)°, V=1713.7(5) A 3 , Z =1, d c =2.193, d m =2.17(2) Mg m −3 . The structure contains a structurally novel Sb 8 Cl 28 4- anion. It is composed of eight deformed octahedra, connected with each other by faces. In cavities formed by inorganic sublattice are located two crystallographically nonequivalent tetramethylammonium cations. One of them is disordered in such a way that all (C, N, H) atoms are split between two positions with occupancy factors 0.5." @default.
- W2044950905 created "2016-06-24" @default.
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- W2044950905 date "2000-11-01" @default.
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- W2044950905 title "Synthesis and structure of tetrakis(tetramethylammonium) octacosachlorooctaantimonate(III) [(CH3)4N]4Sb8Cl28" @default.
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- W2044950905 doi "https://doi.org/10.1016/s0022-2860(00)00600-1" @default.
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